Open Access

Morphology and Structural Studies of Multi-walled Carbon Nanotubes by Spray Pyrolysis using Madhuca Longifolia Oil

S. Karthikeyan, environkarthi@gmail.com
Department of Chemistry, Chikkanna Government Arts College, Tirupur, TN, India.
S. Kalaiselvan, Department of Chemistry, Hindusthan College of Engineering, Coimbatore, TN, India D. Manorangitham, Department of Chemistry, Chikkanna Government Arts College, Tirupur, TN, India. S. Maragathamani Department of Chemistry, Chikkanna Government Arts College, Tirupur, TN, India.


J. Environ. Nanotechnol., Volume 2, No 4 (2013) pp. 15-20

https://doi.org/10.13074/jent.2013.12.132040

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Abstract

Multi-walled carbon nanotubes were synthesized using methyl ester of Madhuca longifolia oil over Fe-Mo impregnated alumina support at 650 °C under N2 atmosphere at normal pressure. Structural characterizations have been done by Field Emission Scanning Electron Microscopy (FESEM), High Resolution Transmission Electron Microscopy (HRTEM) and Raman Spectroscopic analysis. We confirmed that well graphitized multi-walled carbon nanotubes were nicely grown on the chosen catalytic supporting material. The diameter of the carbon nanotubes obtained were between 30 and 40 nm.

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Reference


Angulakshmi, V. S., Sivakumar, N. and Karthikeyan, S., Response surface methodology for optimizing process  parameters  for  synthesis  of  carbon nanotubes,  J.  Environ. Nanotechnol.,  1(1),  40-45( 2012 ).  

http://dx.doi.org/10.13074/jent.2012.10.121019.


Angulakshmi, V. S., Sathiskumar, C. and Karthikeyan, S., Synthesis of multiwalled carbon nanotubes from glycine max oil and their potential applications, J. Environ. Nanotechnol., 2, 101-106(2013). 

http://dx.doi.org/10.13074/jent.2013.02.nciset316.

Brukh, R., Mitra, S., Mechanism of carbon nanotube growth by CVD, Chem. Phys. Lett., 424 126(2006). 

http://dx.doi.org/10.1016/j.cplett.2006.04.028 

Chen, X. Q., Motojima, S., Iwanaga, H., Carbon coatings on carbon micro-coils by pyrolysis of methane and their properties, Carbon, 37, 1825(1999).

http://http://dx.doi.org/10.1016/S0008-6223(99)00056-1 

Dresslhaus, M. S., Dresslhaus, G., Eklund, P. C., Science of fullerenes and carbon nanotubes, Academic press, San Diego, (1996).

Iijima, S., Helical microtubules of graphitic carbon, Nature., 354, 56-58(1991).

http://dx.doi.org/10.1038/354056a0

Karthikeyan,  S.  and  Mahalingam,  P.  Synthesis  and characterization of multiwalled carbon nanotubes from bio-diesel oil: green nanotechnology route, Int.  J.  Gr een.  Nanotechnol., 2(2),  39-4 6 ( 2 0 1 0 ) . 

http://h t t p : / / d x . d o i . o r g / 1 0 . 1 0 8 0 /19430876.2010.532421.

Kumar, M., Ando, Y., Camphor-a botanical precursor producing garden of carbon nanotubes, Diam.Relat. Mater., 12, 998(2003).

http://dx.doi.org/10.1016/S0925-9635(02)00341-2

Lee, M. H., Park, D. G., Preparation of MgO with High Surface Area, and Modification of Its Pore Characteristics, Bull. Korean Chem. Soc., 24, 1437(2003).

Li, Y., Zhang X. B., Tao, X. Y., Growth mechanism of multi-walled carbon nanotubes with or without bundles by catalytic deposition of methane on Mo/MgO, Chem. Phys. Lett., 386, 105(2004) .

http://dx.doi.org/10.1016/j.cplett.2003.12.128 

Luo, T., Liu, J. W., Chen, L. Y., Synthesis of helically coiled carbon nanotubes by reducing ethyl ether with metallic zinc, Carbon, 43, 755(2005).

http://dx.doi.org/10.1016/j.carbon.2004.10.048 

Mageswari, S., Jafar Ahamed, A. and Karthikeyan, S., Effect  of  temperature  and  flowrate of carbon sources  of  multiwalled  car bon  nanotubes synthesized  using  natural  precursor by spray pyrolysis,   J.  Environ.  Nanotechnol.,  1(1),  28-31( 2012 ).

http://dx.doi.org/10.13074/jent.2012.10.121015.

Oberlin, A., Endo, M., Koyama, T., Filamentous growth of carbon through benzene decomposition, J. Cryst. Growth, 32335-32349(1976) .

http://http://dx.doi.org/10.1016/0022-0248(76)90115-9

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