pH-Tuned Synthesis of Samarium-Doped MoO₃/SiO₂ Nanocomposite for Enhanced Electrochemical Performance
J. Environ. Nanotechnol., Volume 13, No 4 (2024) pp. 226-231
Abstract
Molybdenum trioxide has emerged as a promising material for various applications due to its semiconducting nature, layered structure, and high redox activity. In this study, we report the preparation, characterization, and electrochemical performance of samarium-doped MoO3/SiO2 synthesized via a wet-chemical approach at different pH levels. A comprehensive investigation was carried out to understand the structural, morphological, optical, and electrochemical properties using X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), UV-Vis spectroscopy, Fourier-transform infrared spectroscopy (FTIR), and cyclic voltammetry (CV). The results reveal the impact of pH and samarium doping on the crystallinity, particle morphology, optical bandgap, and charge storage properties of MoO3. This study highlights the potential of tailored MoO3-based materials for applications in catalysis, energy storage, and environmental remediation.
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